Iranian chemical communication 2423-4958 2 Issue 2, pp. 82-163, Serial No. 3 2014 04 01 Efficient classical synthesis of aminoazines under microwave irradiation 157 163 666 EN Seyed Mohammad Vahdat Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran Abbas Mohammadzadeh Chemistry Research Laboratory, Faculty of Science,Ayatollah Amoli Branch, Islamic Azad University, Amol, Iran Esmaiel Derafshian Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran Somaieh Akhoondi Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran Journal Article 2014 01 15 In the present study, Aminoazines were prepared from the reaction of amidrazone hydroiodide with various aromatic aldehydes in the presence of a solid base under microwave irradiation with power level of 850 W for 2-7 min in high yields. The amidrazone hydroiodide can also be prepared by the reaction of S-methyl isothiobenzamide hydroiodide and hydrazine in methanol under nitrogen gas. All synthesized compounds were characterized on the basis of IR and 1H NMR spectral data. The significant features of this method are short reaction times, high yields of the products, solvent free reaction, easy work-up procedure, directly production of aminoazines. https://icc.journals.pnu.ac.ir/article_666_9aeaea39104de5c60dee69251ee42838.pdf