Organic chemistry
A green and highly effective protocol for the synthesis of N,N′-alkylidene bisamides using saccharin-N-sulfonic acid

Abdolkarim Zare; Manije Dianat; Nasrin Pishahang; Roghayyeh Khanivar; Soheila Kaman-Torki; Fatemeh Fakhraei; Zahra Kordrostami; Masoud Sadeghei-Takallo

Volume 8, Issue 1 , January 2020, , Pages 58-66

https://doi.org/10.30473/icc.2019.44250.1514

Abstract
  A green and highly effective solvent-free protocol has been reported for the synthesis of N,N′-alkylidene bisamides via the reaction of arylaldehydes (1 eq.) with primary amides (2 eq.) in the presence of saccharin-N-sulfonic acid (SaSA) as a solid-acid catalyst. The mentioned compounds have been ...  Read More

A green and highly effective protocol for the synthesis of N,N′-alkylidene bisamides using saccharin-N-sulfonic acid


Analytical chemistry
Simultaneous determination of sunset yellow and tartrazine in soft drinks samples using nanocrystallites of spinel ferrite- modified electrode

Masoumeh Taei; Hossein Salavati; Masoud Fouladgar; Elmira Abbaszadeha

Volume 8, Issue 1 , January 2020, , Pages 67-79

https://doi.org/10.30473/icc.2019.45932.1543

Abstract
  The ZnCrFeO4 nanoparticles were synthesized as antiferromagnetic material using sol-gel method. The X-ray diffraction (XRD) analysis and transmission electron microscopy (TEM) certified that ZnCrFeO4 nanoparticles have single-phase cubic structure with a range of 50–100 nm in size. A facile and ...  Read More

Simultaneous determination of sunset yellow and tartrazine in soft drinks samples using nanocrystallites of spinel ferrite- modified electrode


Organic chemistry
An efficient and one-pot green synthesis of 2-arylsubstituted benzimidazoles catalyzed by nano-Fe3O4@silica sulfuric acid as a recyclable nanomagnetic solid acid catalyst

Mehdi Fallah-Mehrjardi; Manizhe Ayazi; Sayed Hossein Banitaba

Volume 8, Issue 1 , January 2020, , Pages 80-91

https://doi.org/10.30473/icc.2019.43207.1493

Abstract
  An efficient and green protocol for the synthesis of 2-arylsubstituted benzimidazoles via a condensation reaction of aromatic aldehydes and 1,2-phenylenediamine using nano-Fe3O4@SiO2-SO3H as a solid acid catalyst in ethanol under reflux conditions has been described. The reactions are completed in short ...  Read More

An efficient and one-pot green synthesis of 2-arylsubstituted benzimidazoles catalyzed by nano-Fe3O4@silica sulfuric acid as a recyclable nanomagnetic solid acid catalyst


Medical and Chemistry
Application of guar gum in electrospun nanofibers as mebendazole drug release controller: a kinetic study and thermodynamics analysis

Fatemeh Tavakoli; Hadi Shafiee; Reza Ghasemikhah

Volume 8, Issue 1 , January 2020, , Pages 92-101

https://doi.org/10.30473/icc.2020.50066.1640

Abstract
  The current study aimed at in vitro investigating the kinetic study and thermodynamic analysis of mebendazole drug released from electrospun cellulose nanofiber in which guar gum is used as a release controller. The nanofibers were fabricated by electrospinning technique. The fibers were boosted by different ...  Read More

Application of guar gum in electrospun nanofibers as mebendazole drug release controller: a kinetic study and thermodynamics analysis


Organic chemistry
Tetra-N-Butyl ammonium hydroxide mediated one-pot synthesis of pyrano [2, 3-d] pyrimidinone derivatives

Vivekanand Jadhav; Mohasim M. Patel

Volume 5, Issue 1, pp. 1-120, Serial No. 14 , January 2017, , Pages 115-120

Abstract
  Tetra-N-Butyl Ammonium Hydroxide was used as a catalyst for one-pot, three component condensation reactions consisting of aromatic aldehydes, malononitrile and barbituric acid in ethanol:water solvent system at 60oC. Current method has major advantages like mild reaction conditions with simple operation, ...  Read More

Tetra-N-Butyl ammonium hydroxide mediated one-pot synthesis of pyrano [2, 3-d] pyrimidinone derivatives


Organic chemistry
Guanidine hydrochloride: An efficient catalyst for the synthesis of 2-hydrazolyl-4-thiazolidinone derivatives under solvent free conditions

Shivaji Sandu Pandit; Sonali Shivaji Pardhe; Yashwant Bhaskar Pandit

Volume 5, Issue 2, pp. 121-236, Serial No. 15 , April 2017, , Pages 227-236

Abstract
  A Highly efficient protocol has been developed for the synthesis of 2-hydrazolyl-4-thiazolidinone derivatives installing a one pot three component coupling reaction of an aromatic aldehyde, thiosemicarbazide and maleic anhydride using guanidine hydrochloride as highly inexpensive and environmentally ...  Read More

Guanidine hydrochloride: An efficient catalyst for the synthesis of 2-hydrazolyl-4-thiazolidinone derivatives under solvent free conditions


Organic chemistry
Reusable Silica supported Perchloric acid and potassium bisulphate as green catalysts for thiocyanation of aromatic compounds under solvent free conditions

Chinna Rajanna Kamatala; Hemanth Sriram Y.; Satish Kumar Mukka; Venkateswarlu Marri; Touheeth Fatima; Sai Sudhakar Mukka; Madhusudan Raju R.

Volume 5, Issue 3, pp. 237-363, Serial No. 16 , July 2017, , Pages 352-363

Abstract
  Reusable silica supported perchloric acid and potassium bisulphate have been prepared and explored as green catalysts for thiocyanation of aromatic compounds under conventional and solvent free microwave assisted conditions. The microwave assisted protocol exhibited remarkable rate accelerations and ...  Read More

Reusable Silica supported Perchloric acid and potassium bisulphate as green catalysts for thiocyanation of aromatic compounds under solvent free conditions


Nanochemistry
Fe2V4O13 assisted hetero-Fenton mineralization of methyl orange under UV-A light irradiation

Kaliyamoorthy Gowthami; Palusamy Suppuraj; Ganesamoorthy Thirunarayanan; Balu Krishnakumar; Abílio José Fraga do Nascimento Sobral; Meenakshisundaram Swaminathan; Inbasekaran Muthuvel

Volume 6, Issue 1, pp. 1-108, Serial No. 18 , January 2018, , Pages 97-108

Abstract
  Fe2V4O13 is prepared and characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR), UV-diffuse reflectance spectroscopy (UV-DRS), high resolution scanning electron microscopy (HR-SEM) using energy dispersive X-ray spectroscopy (EDX) analysis. The hetero-Fenton catalyst can be used ...  Read More

Fe2V4O13 assisted hetero-Fenton mineralization of methyl orange under UV-A light irradiation


Au nano dendrites/composition optimized Nd-dopped cobalt oxide as an efficient electrocatalyst for ethanol oxidation

Foroozan Hasanpour; Masoumeh Taei; Masoud Fouladgar; Mehdi Salehi

Volume 8, Issue 1 , January 2020, , Pages 102-111

https://doi.org/10.30473/icc.2020.9788

Abstract
  In this study, Nd-doped cobalt oxide (Nd-Co3O4) nanoparticles were prepared by a combustion synthesis procedure using Co(acac)3 complex. The nanoparticles were characterized by infrared spectroscopy (IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy ...  Read More

Au nano dendrites/composition optimized Nd-dopped cobalt oxide as an efficient electrocatalyst for ethanol oxidation


Synthesis and characterization of MCM-41@L-Arginine@Pd(0) and its excellent catalytic activity as recyclable heterogeneous catalyst for Suzuki-Miyaura cross-coupling reaction

Somayeh Nazarzadeh; Arash Ghorbani-Choghamarani; Elham Tahanpesar

Volume 7, Issue 4. pp. 230-306, Serial No. 25 , October 2019, , Pages 295-306

https://doi.org/10.30473/icc.2019.41086.1454

Abstract
  MCM-41@L-Arg@Pd(0) has been prepared by some consequence reactions. This nano structural material has been characterized via different technique including: XRD, TGA, BET, EDS, X-Ray maps, SEM, ICP-OES and FT-IR analysis. The synthesis of a variety of biphenyl compounds has been achieved successfully ...  Read More